| 1. Identity statement | |
| Reference Type | Journal Article |
| Site | mtc-m16.sid.inpe.br |
| Holder Code | isadg {BR SPINPE} ibi 8JMKD3MGPCW/3DT298S |
| Identifier | 6qtX3pFwXQZsFDuKxG/GEA34 |
| Repository | sid.inpe.br/marciana/2005/07.05.12.06 (restricted access) |
| Last Update | 2005:07.05.03.00.00 (UTC) administrator |
| Metadata Repository | sid.inpe.br/marciana/2005/07.05.12.07 |
| Metadata Last Update | 2018:06.05.01.16.46 (UTC) administrator |
| Secondary Key | INPE-12856-PRE/8146 |
| ISSN | 0925-9635 |
| Citation Key | FerreiraAzBeAmAlOlSi:2005:NaFiGr |
| Title | Nanodiamond films growth on porous silicon substrates for electrochemical applications  |
| Year | 2005 |
| Month | Mar-Jul |
| Access Date | 2024, May 12 |
| Secondary Type | PRE PI |
| Number of Files | 1 |
| Size | 742 KiB |
| 2. Context | |
| Author | 1 Ferreira, Neidenei Gomes 2 Azevedo, Adriana Faria 3 Beloto, Antonio Fernando 4 Amaral, M. 5 Almeida, F. A. 6 Oliveira, F. J. 7 Silva, R. F. |
| Resume Identifier | 1 8JMKD3MGP5W/3C9JHU3 2 3 8JMKD3MGP5W/3C9JGJ8 |
| Group | 1 LAS-INPE-MCT-BR |
| Affiliation | 1 Instituto Nacional de Pesquisas Espaciais, Laboratorio Associado de Sensores e Materiais (INPE, LAS) 2 Univ Aveiro, Dept Engn Ceram & Vidro, Aveiro, P-3800 Portugal |
| Journal | Diamond and Related Materials |
| Volume | 14 |
| Number | 3-7 |
| Pages | 441-445 |
| History (UTC) | 2005-07-05 12:07:00 :: sergio -> administrator :: 2006-09-28 22:31:40 :: administrator -> sergio :: 2008-01-07 12:54:03 :: sergio -> administrator :: 2018-06-05 01:16:46 :: administrator -> marciana :: 2005 |
| 3. Content and structure | |
| Is the master or a copy? | is the master |
| Content Stage | completed |
| Transferable | 1 |
| Content Type | External Contribution |
| Keywords | nanocrystalline diamond porous electrode cyclic voltammetry / DOPED DIAMOND ELECTRODES CHEMICAL-VAPOR-DEPOSITION CARBON-FIBER CLOTHS POLYCRYSTALLINE DIAMOND EFFICIENCY MECHANISM OXIDATION |
| Abstract | Nanocrystalline diamond (NCD) films were successfully grown on micrometric porous silicon (PS) substrate in a hot filament chemical vapor deposition (HFCVD) reactor. The films were deposited at substrate temperature of 920 K and 6.5 kPa, after seeding pretreatment. The gas flow rate was set in a 50 seem for Ar-CH4-H-2 Mixture. PS substrates were produced by anodic etching using n-type silicon wafers. The morphology, quality and electrochemical response of NCD have been analyzed by scanning electron microscopy (SEM), Raman scattering spectroscopy and cyclic voltammetry (CV) measurements. SEM images have shown faceted nanograins with average size from 30 to 50 nm and uniform surface texture covering all the supports among the pores resulting in an apparent micro honeycomb structure. Raman spectra have exhibited a shoulder at 1550 cm(-1) that is NCD characteristic and have confirmed the good quality films with diamond purity around 90%. Electrochemical response and capacitance behavior of NCD/PS electrodes immersed in aqueous electrolyte solution without redox-active reagents has been explored. The work potential window remains large for NCD, in a similar way of boron doped diamond (BDD), but with a large capacitive background current compared to BDD. NCD/PS presented capacitance values from 230 to 990 mu F cm(-2), while such capacitance values for BDD were between 20 and 40 mu F cm(-2) in the potential range of -0.5 up to 1.0 V x Ag/AgCl. (c) 2005 Elsevier B.V. All rights reserved. . |
| Area | FISMAT |
| Arrangement | urlib.net > BDMCI > Fonds > Produção anterior à 2021 > LABAS > Nanodiamond films growth... |
| doc Directory Content | access |
| source Directory Content | there are no files |
| agreement Directory Content | there are no files |
| 4. Conditions of access and use | |
| Language | en |
| Target File | nanodiamond films.pdf |
| User Group | administrator sergio |
| Visibility | shown |
| Copy Holder | SID/SCD |
| Archiving Policy | denypublisher denyfinaldraft24 |
| Read Permission | deny from all and allow from 150.163 |
| 5. Allied materials | |
| Next Higher Units | 8JMKD3MGPCW/3ESR3H2 |
| Dissemination | WEBSCI; PORTALCAPES; COMPENDEX. |
| Host Collection | sid.inpe.br/banon/2003/08.15.17.40 |
| 6. Notes | |
| Empty Fields | alternatejournal archivist callnumber copyright creatorhistory descriptionlevel documentstage doi e-mailaddress electronicmailaddress format isbn label lineage mark mirrorrepository nextedition notes orcid parameterlist parentrepositories previousedition previouslowerunit progress project readergroup rightsholder schedulinginformation secondarydate secondarymark session shorttitle sponsor subject tertiarymark tertiarytype typeofwork url versiontype |
| 7. Description control | |
| e-Mail (login) | marciana |
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